Assessing dimerisation degree and cooperativity in a biomimetic small-molecule model by pulsed EPR
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Pulsed electron paramagnetic resonance (EPR) spectroscopy is gaining increasing importance as a complementary biophysical technique in structural biology. Here, we describe the synthesis, optimisation, and EPR titration studies of a spin-labelled terpyridine Zn(II) complex serving as a small-molecule model system for tuneable dimerisation.
Ackermann , K , Giannoulis , A , Cordes , D B , Slawin , A M Z & Bode , B E 2015 , ' Assessing dimerisation degree and cooperativity in a biomimetic small-molecule model by pulsed EPR ' Chemical Communications , vol 51 , pp. 5257-5260 . DOI: 10.1039/C4CC08656B
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