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Crystal structure of 2-benzoylamino-it N'-(4-hydroxybenzylidene)-3-(thiophen-2-yl)prop-2-enohydrazide

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Glidewell_2016_ACECC_CrystalStructure_CC.pdf (852.7Kb)
Date
01/08/2016
Author
Subbulakshmi, Karanth N.
Narayana, Badiadka
Yathirajan, Hemmige S.
Jasinski, Jerry P.
Rathore, Ravindranath S.
Glidewell, Christopher
Keywords
Crystal structure
Supramolecular structure
Molecular conformation
Hydrogen bonding
QD Chemistry
DAS
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Abstract
In the title compound, C21H17N3O3S, the non-H atoms, apart from those in the benzoyl group, are almost coplanar (r.m.s. deviation = 0.049 Å) and the benzoyl group is almost orthogonal to the plane of the rest of the molecule [dihedral angle = 80.34(6)º]. In the crystal, a combination of N---H···O and asymmetric bifurcated O---H···(N,O) hydrogen bonds link the molecules into a three-dimensional network. Weak C---H···O interactions are also observed.
Citation
Subbulakshmi , K N , Narayana , B , Yathirajan , H S , Jasinski , J P , Rathore , R S & Glidewell , C 2016 , ' Crystal structure of 2-benzoylamino-it N ' -(4-hydroxybenzylidene)-3-(thiophen-2-yl)prop-2-enohydrazide ' , Acta Crystallographica Section E , vol. 72 , no. 8 , pp. 1099-1102 . https://doi.org/10.1107/S2056989016010975
Publication
Acta Crystallographica Section E
Status
Peer reviewed
DOI
https://doi.org/10.1107/S2056989016010975
ISSN
2056-9890
Type
Journal article
Rights
This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
Description
JPJ acknowledges the NSF–MRI program (grant No. 1039027) for funds to purchase the X-ray diffractometer.
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  • University of St Andrews Research
URI
http://hdl.handle.net/10023/9541

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