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dc.contributor.authorTran, F.
dc.contributor.authorLancefield, C. S.
dc.contributor.authorKamer, P. C. J.
dc.contributor.authorLebl, T.
dc.contributor.authorWestwood, N. J.
dc.date.accessioned2015-02-02T16:01:02Z
dc.date.available2015-02-02T16:01:02Z
dc.date.issued2015-01-01
dc.identifier.citationTran , F , Lancefield , C S , Kamer , P C J , Lebl , T & Westwood , N J 2015 , ' Selective modification of the β-β linkage in DDQ-treated Kraft lignin analysed by 2D NMR spectroscopy ' , Green Chemistry , vol. 17 , no. 1 , pp. 244-249 . https://doi.org/10.1039/C4GC01012Den
dc.identifier.issn1463-9262
dc.identifier.otherPURE: 154416662
dc.identifier.otherPURE UUID: 6c26bdad-0908-4f71-abdf-8545d979a9f7
dc.identifier.otherBibtex: urn:6aca4da47efc64ce614ee3569f4caf6d
dc.identifier.otherWOS: 000346742600023
dc.identifier.otherScopus: 85009806507
dc.identifier.otherORCID: /0000-0002-0269-3221/work/48131735
dc.identifier.otherORCID: /0000-0003-0630-0138/work/56424198
dc.identifier.urihttps://hdl.handle.net/10023/6056
dc.descriptionThis work was funded by the EPSRC grants EP/J018139/1 and EP/K00445X/1en
dc.description.abstractThe depolymerisation of the biopolymer lignin has the potential to provide access to a range of high value and commodity chemicals. However, research in this increasingly important area of green chemistry is hindered by the lack of analytical methods. The key challenge in using NMR is the throughput that can be achieved without the need for high field spectrometers fitted with cryoprobes. Here, we report the use of a relatively fast 2D HSQC NMR experiment performed on a 500 MHz spectrometer fitted with a BBFO+ probe to obtain high quality spectra. The use of the developed protocol to study the selective modification of the β-β linkage in Kraft lignin is also reported.
dc.format.extent6
dc.language.isoeng
dc.relation.ispartofGreen Chemistryen
dc.rights© The Authors 2015. This article is licensed under a Creative Commons Attribution 3.0 Unported Licence (http://creativecommons.org/licenses/by/3.0/)en
dc.subjectQD Chemistryen
dc.subjectNDASen
dc.subject.lccQDen
dc.titleSelective modification of the β-β linkage in DDQ-treated Kraft lignin analysed by 2D NMR spectroscopyen
dc.typeJournal articleen
dc.contributor.sponsorEPSRCen
dc.contributor.sponsorEPSRCen
dc.contributor.sponsorEPSRCen
dc.description.versionPublisher PDFen
dc.contributor.institutionUniversity of St Andrews. School of Chemistryen
dc.contributor.institutionUniversity of St Andrews. EaSTCHEMen
dc.contributor.institutionUniversity of St Andrews. Biomedical Sciences Research Complexen
dc.identifier.doihttps://doi.org/10.1039/C4GC01012D
dc.description.statusPeer revieweden
dc.identifier.urlhttp://www.rsc.org/suppdata/gc/c4/c4gc01012d/c4gc01012d1.pdfen
dc.identifier.grantnumberEP/K00445X/1en
dc.identifier.grantnumberEP/J018139/1en
dc.identifier.grantnumberEP/J018139/1en


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