(8RS)-4-Amino-6-(4-chlorophenyl)-8-(2,4-dichlorothiazol-5-yl)-8, 9-dihydro-7H-pyrimido[4,5-b][1,4]diazepine N,N-dimethylformamide monosolvate : sheets built from N-H⋯N and C-H⋯O hydrogen bonds
Abstract
In the title compound, C16H11Cl3N6S·C3H7NO, the seven-membered ring adopts a conformation which is close to the twist-boat form. The molecular components are linked into sheets by a combination of two N-H⋯N hydrogen bonds and two C-H⋯O hydrogen bonds. Comparisons are made with other aminopyrimidine derivatives.
Citation
Ramírez , J , Insuasty , B , Cobo , J & Glidewell , C 2014 , ' (8RS)-4-Amino-6-(4-chlorophenyl)-8-(2,4-dichlorothiazol-5-yl)-8, 9-dihydro-7H-pyrimido[4,5-b][1,4]diazepine N,N-dimethylformamide monosolvate : sheets built from N-H⋯N and C-H⋯O hydrogen bonds ' Acta Crystallographica Section C Structural Chemistry , vol 70 , no. 6 , pp. 536-540 . DOI: 10.1107/S2053229614008936
Version
Publisher PDF
Publication
Acta Crystallographica Section C Structural Chemistry
Status
Peer reviewed
URI
http://hdl.handle.net/10023/5256http://www.scopus.com/inward/record.url?eid=2-s2.0-84905500772&partnerID=8YFLogxK
ISSN
2053-2296Type
Journal article
Rights
© 2014 International Union of Crystallography.
Description
The authors thank the Centro de Instrumentación Científico-Técnica of the Universidad de Jaén and the staff for the data collection. Financial support from COLCIENCIAS, the Universidad del Valle, the Consejería de Economía, Innovación, Ciencia y Empleo (Junta de Andalucía, Spain) and the Universidad de Jaén is gratefully acknowledged.
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