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(5RS)-5-(4-Methoxyphenyl)-2-(methylsulfanyl)benzo[g]pyrimido[4,5-b]quinoline-4,6,11(3H,5H,12H)-trione, with Z '=3, forms a three-dimensional hydrogen-bonded framework containing five types of hydrogen bond

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dc.contributor.authorCastillo, Yelder A.
dc.contributor.authorZapata, Luis F.
dc.contributor.authorTrilleras, Jorge
dc.contributor.authorCobo, Justo
dc.contributor.authorGlidewell, Christopher
dc.date.accessioned2014-08-27T10:31:03Z
dc.date.available2014-08-27T10:31:03Z
dc.date.issued2014-01
dc.identifier143710344
dc.identifier489b0562-714d-4d97-9e6c-e9b9aeaf7d18
dc.identifier000331291400013
dc.identifier84901911054
dc.identifier000331291400013
dc.identifier.citationCastillo , Y A , Zapata , L F , Trilleras , J , Cobo , J & Glidewell , C 2014 , ' (5RS)-5-(4-Methoxyphenyl)-2-(methylsulfanyl)benzo[g]pyrimido[4,5-b]quinoline-4,6,11(3H,5H,12H)-trione, with Z '=3, forms a three-dimensional hydrogen-bonded framework containing five types of hydrogen bond ' , Acta Crystallographica Section C: Crystal Structure Communications , vol. 70 , pp. 50-54 . https://doi.org/10.1107/S2053229613032956en
dc.identifier.issn0108-2701
dc.identifier.urihttps://hdl.handle.net/10023/5251
dc.descriptionThe authors thank ‘Centro de Instrumentacion Cientıfico-Tecnica of Universidad de Jaen’ and the staff for data collection. YAC, LFZ and JT thank the Universidad del Atlantico and ‘Fundacion para la Promocion de la Investigacion y la Tecnologıa – Banco de la Republica’ Proyecto No. 2.627, Convenio No. 201001, for financial support. JC thanks the Consejerıa de Innovacion, Ciencia y Empresa (Junta de Andalucıa, Spain) and the Universidad de Jaen for financial support.en
dc.description.abstractThe title compound, C23H17N3O4S, crystallizes with Z' = 3 in the space group P. Two of the three independent molecules are broadly similar in terms of both their molecular conformations and their participation in hydrogen bonds, but the third molecule differs from the other two in both of these respects. The molecules are linked by a combination of N-HO, N-HN, C-HO, C-HN and  C-H(arene) hydrogen bonds to form a continuous three-dimensional framework structure within which a centrosymmetric six-molecule aggregate can be identified as a key structural element.
dc.format.extent19
dc.format.extent892202
dc.language.isoeng
dc.relation.ispartofActa Crystallographica Section C: Crystal Structure Communicationsen
dc.subjectcrystal structureen
dc.subjecthydrogen bondingen
dc.subjectsupramolecular aggregationen
dc.subjectsix-molecule aggregateen
dc.subjectPhenylphosphonic aciden
dc.subject4,4'-sulfonyldiphenolen
dc.subject4,4'-thiodiphenolen
dc.subjectDerivativesen
dc.subjectAdductsen
dc.subjectAgentsen
dc.subjectRADIIen
dc.subjectVANen
dc.subjectQD Chemistryen
dc.subject.lccQDen
dc.title(5RS)-5-(4-Methoxyphenyl)-2-(methylsulfanyl)benzo[g]pyrimido[4,5-b]quinoline-4,6,11(3H,5H,12H)-trione, with Z '=3, forms a three-dimensional hydrogen-bonded framework containing five types of hydrogen bonden
dc.typeJournal articleen
dc.contributor.institutionUniversity of St Andrews. School of Chemistryen
dc.identifier.doi10.1107/S2053229613032956
dc.description.statusPeer revieweden
dc.identifier.urlhttp://scripts.iucr.org/cgi-bin/sendsup?yf3052en


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