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dc.contributor.authorTrilleras, J.
dc.contributor.authorUtria, M.
dc.contributor.authorCobo, J.
dc.contributor.authorGlidewell, C.
dc.date.accessioned2014-08-27T10:01:07Z
dc.date.available2014-08-27T10:01:07Z
dc.date.issued2014-02-01
dc.identifier.citationTrilleras , J , Utria , M , Cobo , J & Glidewell , C 2014 , ' (E)-1-[(5-Chloro-3-methyl-1-phenyl-1H-pyrazol-4-yl)methylidene] -2-phenylhydrazine : sheets built from π-stacked hydrogen-bonded chains ' , Acta Crystallographica Section C: Crystal Structure Communications , vol. 70 , no. 2 , pp. 216-219 . https://doi.org/10.1107/S2053229614000680en
dc.identifier.issn0108-2701
dc.identifier.otherPURE: 143707841
dc.identifier.otherPURE UUID: d0924c1a-7911-4dc2-8575-499596899905
dc.identifier.otherScopus: 84901483745
dc.identifier.otherWOS: 000332218000022
dc.identifier.urihttps://hdl.handle.net/10023/5248
dc.descriptionThe authors thank `Centro de Instrumentación Científico-Técnica of Universidad de Jaén' and the staff for data collection. JT and MU thank UNIATLANTICO (Universidad del Atlántico, Colombia) for financial support. JC thanks the Consejería de Innovación, Ciencia y Empresa (Junta de Andalucía, Spain) and the Universidad de Jaén for financial support.en
dc.description.abstractThe reaction between 5-chloro-3-methyl-1-phenyl-1H-pyrazole-4-carbaldehyde and phenylhydrazine proceeds via condensation to provide the title compound, C17H15ClN4, (I), rather than via the alternative routes of simple nucleophilic substitution or cyclocondensation. With the exception of the phenyl group bonded directly to the pyrazole ring, the non-H atoms of (I) are nearly coplanar, with an r.m.s. deviation of 0.058Å. The molecules are linked into C(7) chains by a single N - H⋯N hydrogen bond, and the chains are linked by π-π stacking interactions to form sheets.
dc.format.extent4
dc.language.isoeng
dc.relation.ispartofActa Crystallographica Section C: Crystal Structure Communicationsen
dc.rights© 2014 International Union of Crystallography.en
dc.subjectCrystal structureen
dc.subjectpi-stacked hydrogen-bonded chainsen
dc.subjectCondensation reactionen
dc.subjectPhenyl­hydrazine derivativeen
dc.subjectQD Chemistryen
dc.subject.lccQDen
dc.title(E)-1-[(5-Chloro-3-methyl-1-phenyl-1H-pyrazol-4-yl)methylidene] -2-phenylhydrazine : sheets built from π-stacked hydrogen-bonded chainsen
dc.typeJournal articleen
dc.description.versionPublisher PDFen
dc.contributor.institutionUniversity of St Andrews. School of Chemistryen
dc.identifier.doihttps://doi.org/10.1107/S2053229614000680
dc.description.statusPeer revieweden
dc.identifier.urlhttp://www.scopus.com/inward/record.url?eid=2-s2.0-84901483745&partnerID=8YFLogxKen
dc.identifier.urlhttp://scripts.iucr.org/cgi-bin/sendsup?cnor=sf3218&type=supplementarymaterialsen


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