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Strategies for equivalent dose determination without heating, suitable for portable luminescence readers

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Roberts_2018_RM_dosedetermination_AAM.pdf (1021.Kb)
Date
27/04/2018
Author
Roberts, H. M.
Duller, G. A. T.
Gunn, M.
Cousins, C.R.
Cross, R. E.
Langstaff, D.
Funder
Science & Technology Facilities Council
Grant ID
ST/P001971/1
Keywords
Quartz
Preheating
Dating
De determination
110C TL peak
GE Environmental Sciences
QC Physics
NDAS
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Abstract
In recent years a number of portable instruments have been built for measuring the optically stimulated luminescence (OSL) signal from naturally occurring minerals. Some of these instruments have incorporated ionising radiation sources, giving the possibility of determining an equivalent dose (De), but little use has been made of these. One challenge has been that heating samples in this type of equipment is a major engineering challenge, yet methods for De determination use thermal pretreatments to remove charge from unstable traps, making signals arising from irradiation in nature and the laboratory comparable. This paper explores three strategies for obtaining accurate estimates of the De of samples in situations where thermal treatments are not possible: (1) deriving a correction factor based on comparing De values obtained using protocols with and without heating; (2) removing the contribution from the 110 °C TL peak and other unstable defects by component fitting the unheated OSL signal; and (3) adding a small beta dose to the sample prior to measurement of the natural luminescence signal so that the 110 °C TL peak is filled, making this measurement comparable with regeneration measurements where this peak is also populated. All three methods are promising when applied to quartz that has been physically separated from samples using standard laboratory procedures. The next step in this work will be to explore whether such methods can be applied to mixed mineral assemblages as would be encountered in the field.
Citation
Roberts , H M , Duller , G A T , Gunn , M , Cousins , C R , Cross , R E & Langstaff , D 2018 , ' Strategies for equivalent dose determination without heating, suitable for portable luminescence readers ' , Radiation Measurements , vol. In press . https://doi.org/10.1016/j.radmeas.2018.04.018
Publication
Radiation Measurements
Status
Peer reviewed
DOI
https://doi.org/10.1016/j.radmeas.2018.04.018
ISSN
1350-4487
Type
Journal article
Rights
© 2018 Elsevier Ltd. This work has been made available online in accordance with the publisher’s policies. This is the author created, accepted version manuscript following peer review and may differ slightly from the final published version. The final published version of this work is available at https://doi.org/10.1016/j.tet.2018.04.086
Description
This work was supported by the UK Space Agency CREST3 program under grant ST/P001998/1. Research in Next Generation Luminescence methods in Aberystwyth is supported by NERC grant CC003, and by HEFCW infrastructure funding for SPARCL.
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URI
http://hdl.handle.net/10023/17596

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