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A minor byproduct in the reaction of (S)-prolinol with thiophosgene in the presence of triethylamine is identified as a novel tricyclic dipyrrolidino-1,3,6-oxadiazocane-2-thione, the first example of such a ring system, and a representative of the uncommon but useful 1,3,6-oxadiazocanes. A mechanism is proposed for its formation.
Aitken , R A & Ali , K 2018 , ' Octahydro-1 H ,5 H ,7 H -dipyrrolo[1,2-c:1',2'- f ][1,3,6]oxadiazocine-5-thione ' , Molbank , vol. 2018 , M993 . https://doi.org/10.3390/M993
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