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An improved procedure for isolation of 5-amino-3-methyl-1,2,4-thiadiazole in pure form on a multi-gram scale without chromatography is reported. Its 1H and 13C NMR and IR data are presented and previously published erroneous data corrected. The molecular structure is confirmed by X-ray diffraction which shows layers consisting of an elaborate two-dimensional hydrogen bonded network of molecules
Aitken , R A & Slawin , A M Z 2018 , ' 5-Amino-3-methyl-1,2,4-thiadiazole ' Molbank , vol 2018 , no. 1 , M977 . DOI: 10.3390/M977
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