5-Amino-3-methyl-1,2,4-thiadiazole

Aitken, R. Alan; Slawin, Alexandra M. Z.

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Date

21/01/2018

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Abstract

An improved procedure for isolation of 5-amino-3-methyl-1,2,4-thiadiazole in pure form on a multi-gram scale without chromatography is reported. Its 1H and 13C NMR and IR data are presented and previously published erroneous data corrected. The molecular structure is confirmed by X-ray diffraction which shows layers consisting of an elaborate two-dimensional hydrogen bonded network of molecules

Citation

Aitken , R A & Slawin , A M Z 2018 , ' 5-Amino-3-methyl-1,2,4-thiadiazole ' , Molbank , vol. 2018 , no. 1 , M977 . https://doi.org/10.3390/M977

Publication

Molbank

Status

Peer reviewed

DOI

https://doi.org/10.3390/M977

ISSN

1422-8599

Type

Journal article

Rights

© 2018 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).

Collections

University of St Andrews Research

URL

http://www.mdpi.com/1422-8599/2018/1/M977#supplementary

URI

http://hdl.handle.net/10023/12556