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5-Amino-3-methyl-1,2,4-thiadiazole

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molbank_2018_M977_SI.pdf (1.566Mb)
Date
21/01/2018
Author
Aitken, R. Alan
Slawin, Alexandra M. Z.
Keywords
1,2,4-thiadiazole
X-ray structure
IR spectrum
NMR spectra
QD Chemistry
DAS
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Abstract
An improved procedure for isolation of 5-amino-3-methyl-1,2,4-thiadiazole in pure form on a multi-gram scale without chromatography is reported. Its 1H and 13C NMR and IR data are presented and previously published erroneous data corrected. The molecular structure is confirmed by X-ray diffraction which shows layers consisting of an elaborate two-dimensional hydrogen bonded network of molecules
Citation
Aitken , R A & Slawin , A M Z 2018 , ' 5-Amino-3-methyl-1,2,4-thiadiazole ' , Molbank , vol. 2018 , no. 1 , M977 . https://doi.org/10.3390/M977
Publication
Molbank
Status
Peer reviewed
DOI
https://doi.org/10.3390/M977
ISSN
1422-8599
Type
Journal article
Rights
© 2018 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
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  • University of St Andrews Research
URL
http://www.mdpi.com/1422-8599/2018/1/M977#supplementary
URI
http://hdl.handle.net/10023/12556

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