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Synthesis and single crystal structures of substituted-1,3-selenazol-2-amines

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dc.contributor.authorHua, Guoxiong
dc.contributor.authorDu, Junyi
dc.contributor.authorSlawin, Alexandra Martha Zoya
dc.contributor.authorWoollins, John Derek
dc.date.accessioned2017-01-10T16:30:11Z
dc.date.available2017-01-10T16:30:11Z
dc.date.issued2016-12-29
dc.identifier.citationHua , G , Du , J , Slawin , A M Z & Woollins , J D 2016 , ' Synthesis and single crystal structures of substituted-1,3-selenazol-2-amines ' , Molecules , vol. 22 , no. 1 , 46 . https://doi.org/10.3390/molecules22010046en
dc.identifier.issn1420-3049
dc.identifier.otherPURE: 248524993
dc.identifier.otherPURE UUID: 2f01838a-2721-48d0-9d74-a373863fcb1e
dc.identifier.otherScopus: 85009811547
dc.identifier.otherORCID: /0000-0002-9527-6418/work/56861733
dc.identifier.otherORCID: /0000-0002-1498-9652/work/31779151
dc.identifier.otherWOS: 000395473500046
dc.identifier.urihttps://hdl.handle.net/10023/10078
dc.descriptionThis article belongs to the Special Issue Celebrating Two Centuries of Research in Selenium Chemistry: State of the Art and New Prospectivesen
dc.description.abstractThe synthesis and X-ray single crystal structures of a series of new 4-substituted-1,3-selenazol-2-amines is reported. The efficient preparation of 4-substituted-1,3-selenazol-2-amines was carried out by two-component cyclization of the selenoureas with equi-molar amounts of α-haloketones. The selenoureas were obtained from the reaction of Woollins’ reagent with cyanamides, followed by hydrolysis with water. All new compounds have been characterized by IR spectroscopy, multi-NMR (1H, 13C, 77Se) spectroscopy, accurate mass measurement and single crystal X-ray structure analysis.
dc.language.isoeng
dc.relation.ispartofMoleculesen
dc.rightsCopyright (c) 2016, the authors. This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. (CC BY 4.0).en
dc.subjectCyanamidesen
dc.subjectWoollins’ reagenten
dc.subjectSelenoureasen
dc.subjectSelenazol-2-aminesen
dc.subjectQD Chemistryen
dc.subjectDASen
dc.subject.lccQDen
dc.titleSynthesis and single crystal structures of substituted-1,3-selenazol-2-aminesen
dc.typeJournal articleen
dc.description.versionPublisher PDFen
dc.contributor.institutionUniversity of St Andrews. School of Chemistryen
dc.contributor.institutionUniversity of St Andrews. Office of the Principalen
dc.contributor.institutionUniversity of St Andrews. EaSTCHEMen
dc.identifier.doihttps://doi.org/10.3390/molecules22010046
dc.description.statusPeer revieweden
dc.identifier.urlhttp://www.mdpi.com/1420-3049/22/1/46/s1en


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