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Highly efficient synthesis of LTA-type aluminophosphate molecular sieve by improved ionothermal method

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ZhouW_NJC_110116.pdf (6.050Mb)
Date
01/03/2016
Author
Zhao, Xinhong
Zhao, Jiangbo
Chiang, Chang-Yang
Li, Zhengshan
Zhao, Yu
Zhou, Wuzong
Funder
EPSRC
Grant ID
EP/F019580/1
Keywords
QD Chemistry
NDAS
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Abstract
LTA-type aluminophosphate molecular sieve has been successfully synthesized by improvedionothermal method from a gel containing low-dosage ionic liquids. The optimum syntheticconditions of this material are refined. The resultant LTA molecular sieves were characterized byXRD, SEM, TG-DTA, CHN elemental analysis, solution 13C NMR, EDX, TEM and N2physisorption. The composition of the resulting LTA-type molecular sieves is determined to be(Al12P12O48)(C4H9NO)2(C8H15N2+)2(F-)2, for which morpholine together with1-butyl-3-methylimidazolium cations act as the structure-directing agent. The high zeolite yield, as well as the high specific surface area and micropore volume for the calcined LTA-type materials imply that these zeolitic materials have a high potential in applications.
Citation
Zhao , X , Zhao , J , Chiang , C-Y , Li , Z , Zhao , Y & Zhou , W 2016 , ' Highly efficient synthesis of LTA-type aluminophosphate molecular sieve by improved ionothermal method ' , New Journal of Chemistry , vol. 40 , no. 3 , pp. 2444-2450 . https://doi.org/10.1039/C5NJ03006D
Publication
New Journal of Chemistry
Status
Peer reviewed
DOI
https://doi.org/10.1039/C5NJ03006D
ISSN
1144-0546
Type
Journal article
Rights
Copyright 2016 the Authors. This work is made available online in accordance with the publisher’s policies. This is the author created, accepted version manuscript following peer review and may differ slightly from the final published version. The final published version of this work is available at: https://dx.doi.org/10.1039/C5NJ03006D
Description
This work was supported by the National Natural Science Foundation of China (Grant No. 21306072, 21203081) and Development Program of Lanzhou University of Technology for excellent teachers (Grant No. Q201113). WZ thanks EPSRC for financial support to upgrade the SEM facilities (No. EP/F019580/1). We cordially thank the Reviewers and Editors for providing us with valuable comments and suggestions.
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  • University of St Andrews Research
URL
http://www.rsc.org/suppdata/c5/nj/c5nj03006d/c5nj03006d1.pdf
URI
http://hdl.handle.net/10023/10066

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